The raw NMR data files for all three T1rho trials at room temperature for the FD31*-Edelta nucleated calcite sample showing almost no mobility for the Glu sidechain carbonyls in FD31* on the millisecond timescale.
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Comparison of frozen and room temperature 1H-13C CP-MAS spectra for FD31-U-T nucleated calcite show that the threonine backbone carbonyl is immobile at both temperatures on the ~500 microsecond timescale. A slight decrease in signal to noise between the room temperature and frozen spectra does...
Raw data for all three trials used to calculate the T1rho value for FD31-U-T nucleated calcite at both room temperature and frozen. This data shows that the FD31 backbone carbonyl in threonine is immobile in nucleated calcite on the millisecond timescale at both temperatures.
Room temperature and frozen CP-MAS spectra of FD31*-Edelta nucleated calcite showing the overall CSA pattern does not change as a function of temperature. The FD31* Glu sidechain carbonyl appears to be mobile on the ~500 microsecond timescale under both temperature conditions.
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